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Second cycle
degree courses
Single cycle
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School of Medicine
CHEMISTRY AND PHARMACEUTICAL TECHNIQUES
Course unit
DRUG ANALYSIS 1 AND ANALYTICAL CHEMISTRY
FAM1026978, A.A. 2019/20

Information concerning the students who enrolled in A.Y. 2019/20

Information on the course unit
Degree course 5 years single cycle degree in
CHEMISTRY AND PHARMACEUTICAL TECHNIQUES
FA1733, Degree course structure A.Y. 2009/10, A.Y. 2019/20
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Number of ECTS credits allocated 8.0
Type of assessment Mark
Course unit English denomination DRUG ANALYSIS 1 AND ANALYTICAL CHEMISTRY
Department of reference Department of Pharmaceutical and Pharmacological Sciences
Mandatory attendance
Language of instruction Italian
Branch PADOVA
Single Course unit The Course unit CANNOT be attended under the option Single Course unit attendance
Optional Course unit The Course unit is available ONLY for students enrolled in CHEMISTRY AND PHARMACEUTICAL TECHNIQUES

Lecturers
Teacher in charge VALERIO DI MARCO CHIM/01
Other lecturers MIRELLA ZANCATO CHIM/08

ECTS: details
Type Scientific-Disciplinary Sector Credits allocated
Basic courses CHIM/01 Analytical Chemistry 4.0
Core courses CHIM/08 Pharmaceutical Chemistry 4.0

Course unit organization
Period Second semester
Year 1st Year
Teaching method frontal

Type of hours Credits Teaching
hours
Hours of
Individual study
Shifts
Practice 1.0 12 13.0 No turn
Laboratory 2.0 30 20.0 No turn
Lecture 5.0 40 85.0 No turn

Calendar
Start of activities 02/03/2020
End of activities 12/06/2020
Show course schedule 2019/20 Reg.2009 course timetable

Examination board
Board From To Members of the board
7 Commissione a.a. 2019/20 01/12/2019 30/09/2020 DI MARCO VALERIO (Presidente)
ZANCATO MIRELLA (Membro Effettivo)

Syllabus
Prerequisites: The student must know general chemistry.
Target skills and knowledge: - solution equilibria in aqueous media, calculation of the equilibrium concentrations in solution
- basics on the chemical quantitative analytical methods
- classical analytical methods: titrations
- principles of statistics applied to anaytical chemistry (chemiometry)
- qualitative chemical analysis, determination of simple compounds
- simple laboratory skills
Examination methods: There are two written exams, one for the "analisi dei medicinali 1" part, the other for the "chimica analitica" part.
The written exam for the "chimica analitica" part will contain 3 exercises (with a total maximum mark of 18) and 13 questions with predefinite answers (with a total mark of 13). The sum of the marks is the mark of the "chimica analitica" part (31 = 30 cum laude).
From these two exams, "chimica analitica" and "analisi dei medicinali 1" part, a mean mark is obtained. This mean mark can be modified (maximum by 1 unit) by the quality of the laboratory activity and of the written reports of this activity.
Assessment criteria: - mark of the two written exams
- reports of the laboratory activity
- laboratory activity
Course unit contents: This course is divided in two parts (and it has two teachers): the "analisi dei medicinali 1" part, and the "chimica analitica" part. the programs for these two parts are the following.

"Analisi dei medicinali 1" part
Good practice and safety in a chemistry laboratory. Safety rules and papers. Introduction to the inorganic qualitative chemical analysis. Simple techniques and operations: mass and volume measurements, solubilization, dilution, preparation of solutions with known concentration, pH measurement, analytically relevant pH buffers. Precipitation, centrifugation, filtration, liquid-liquid extraction, crystalization. Coordination compounds: introduction and analytical importance. Optical methods: flame tests, atomic absorption spectroscopy, elemental analysis. Main chemical reactions for the identification of unknown compounds.

"Chimica analitica" part
Solution equilibria: acid-base, complexometric, precipitation, redox. Competitive equilibria. Distribution diagrams. Pharmaceutical applications. Objectives and methods of quantitative analytical chemistry. Gravimetric analysis. Titrations (acid-base, complexometric, precipitation, redox). Equivalence point, colorimetric indication and potentiometric (by electrode) indication. Electrodes. Mean, standard deviation, confidence interval and degree, Student and gaussian distribution. Significant digits. Error propagation.
Planned learning activities and teaching methods: There will be theoretical lessons and experimental activities. The former represent the theoretical basis, the latter the practical application. The laboratory activity will be performed both as alone and in groups of more students.
Additional notes about suggested reading: Textbooks:
- V. Di Marco, P. Pastore, G.G. Bombi, Chimica Analitica, ed. Edises, 2015
- A. Araneo, Chimica analitica Qualititiva Metodo periodale, IIIĀ° edition. Editor: Ambrosiana.

There are also slides and written handouts given by the teachers
Textbooks (and optional supplementary readings)
  • V. Di Marco, Pastore P., Bombi, G.G., Chimica analitica: trattazione algebrica e grafica degli equilibri chimici in soluzione acquosa. Napoli: EdiSES, 2015. Cerca nel catalogo
  • A. Araneo, Chimica analitica Qualititiva Metodo periodale. --: Ambrosiana, --. III edizione Cerca nel catalogo

Innovative teaching methods: Teaching and learning strategies
  • Laboratory
  • Working in group
  • Loading of files and pages (web pages, Moodle, ...)

Innovative teaching methods: Software or applications used
  • Moodle (files, quizzes, workshops, ...)

Sustainable Development Goals (SDGs)
Good Health and Well-Being Quality Education