First cycle
degree courses
Second cycle
degree courses
Single cycle
degree courses
School of Medicine
Course unit
FAM1026978, A.A. 2017/18

Information concerning the students who enrolled in A.Y. 2017/18

Information on the course unit
Degree course 5 years single cycle degree in
FA1733, Degree course structure A.Y. 2009/10, A.Y. 2017/18
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Number of ECTS credits allocated 8.0
Type of assessment Mark
Course unit English denomination DRUG ANALYSIS 1 AND ANALYTICAL CHEMISTRY
Department of reference Department of Pharmaceutical and Pharmacological Sciences
E-Learning website
Mandatory attendance
Language of instruction Italian
Single Course unit The Course unit CANNOT be attended under the option Single Course unit attendance
Optional Course unit The Course unit is available ONLY for students enrolled in CHEMISTRY AND PHARMACEUTICAL TECHNIQUES

Teacher in charge MIRELLA ZANCATO CHIM/08
Other lecturers VALERIO DI MARCO CHIM/01

ECTS: details
Type Scientific-Disciplinary Sector Credits allocated
Basic courses CHIM/01 Analytical Chemistry 4.0
Core courses CHIM/08 Pharmaceutical Chemistry 4.0

Course unit organization
Period Second semester
Year 1st Year
Teaching method frontal

Type of hours Credits Teaching
Hours of
Individual study
Practice 1.0 12 13.0 No turn
Laboratory 2.0 30 20.0 No turn
Lecture 5.0 40 85.0 No turn

Start of activities 26/02/2018
End of activities 01/06/2018
Show course schedule 2019/20 Reg.2009 course timetable

Examination board
Board From To Members of the board
7 Commissione a.a. 2019/20 01/12/2019 30/09/2020 DI MARCO VALERIO (Presidente)
ZANCATO MIRELLA (Membro Effettivo)
6 Commissione a.a. 2018/19 01/12/2018 30/09/2019 ZANCATO MIRELLA (Presidente)
DI MARCO VALERIO (Membro Effettivo)
5 Commissione a.a. 2017/18 01/12/2017 30/09/2018 ZANCATO MIRELLA (Presidente)
DI MARCO VALERIO (Membro Effettivo)

Prerequisites: The student must know general chemistry.
Target skills and knowledge: - solution equilibria in aqueous media, calculation of the equilibrium concentrations in solution
- basics on the chemical quantitative analytical methods
- classical analytical methods: titrations
- principles of statistics applied to anaytical chemistry (chemiometry)
- qualitative chemical analysis, determination of simple compounds
- simple laboratory skills
Examination methods: There are two written exams, one for the "analisi dei medicinali 1" part, the other for the "chimica analitica" part. From these two exams, a mean mark is obtained. This mean mark can be modified (maximum by 1 unit) by the quality of the laboratory activity and of the written reports of this activity.
Assessment criteria: - mark of the two written exams
- reports of the laboratory activity
- laboratory activity
Course unit contents: This course is divided in two parts (and it has two teachers): the "analisi dei medicinali 1" part, and the "chimica analitica" part. the programs for these two parts are the following.

"Analisi dei medicinali 1" part
Good practice and safety in a chemistry laboratory. Safety rules and papers. Introduction to the inorganic qualitative chemical analysis. Simple techniques and operations: mass and volume measurements, solubilization, dilution, preparation of solutions with known concentration, pH measurement, analytically relevant pH buffers. Precipitation, centrifugation, filtration, liquid-liquid extraction, crystalization. Coordination compounds: introduction and analytical importance. Optical methods: flame tests, atomic absorption spectroscopy, elemental analysis. Main chemical reactions for the identification of unknown compounds.

"Chimica analitica" part
Solution equilibria: acid-base, complexometric, precipitation, redox. Competitive equilibria. Distribution diagrams. Pharmaceutical applications. Objectives and methods of quantitative analytical chemistry. Gravimetric analysis. Titrations (acid-base, complexometric, precipitation, redox). Equivalence point, colorimetric indication and potentiometric (by electrode) indication. Electrodes. Mean, standard deviation, confidence interval and degree, Student and gaussian distribution. Significant digits. Error propagation.
Planned learning activities and teaching methods: There will be theoretical lessons and experimental activities. The former represent the theoretical basis, the latter the practical application. The laboratory activity will be performed both as alone and in groups of more students.
Additional notes about suggested reading: Textbooks:
- V. Di Marco, P. Pastore, G.G. Bombi, Chimica Analitica, ed. Edises, 2015
- A. Araneo, Chimica analitica Qualititiva Metodo periodale, IIIĀ° edition. Editor: Ambrosiana.

There are also slides and written handouts given by the teachers
Textbooks (and optional supplementary readings)
  • V. Di Marco, Pastore P., Bombi, G.G., Chimica analitica: trattazione algebrica e grafica degli equilibri chimici in soluzione acquosa. Napoli: EdiSES, 2015. Cerca nel catalogo
  • A. Araneo, Chimica analitica Qualititiva Metodo periodale. --: Ambrosiana, --. III edizione Cerca nel catalogo