First cycle
degree courses
Second cycle
degree courses
Single cycle
degree courses
School of Medicine
PHARMACY
Course unit
PRELIMINARY LABORATORY TO DRUG ANALYSIS (Iniziali cognome A-L)
FAO2043780, A.A. 2015/16

Information concerning the students who enrolled in A.Y. 2014/15

Information on the course unit
Degree course 5 years single cycle degree in
PHARMACY
FA1732, Degree course structure A.Y. 2009/10, A.Y. 2015/16
A1301
bring this page
with you
Number of ECTS credits allocated 6.0
Type of assessment Mark
Course unit English denomination PRELIMINARY LABORATORY TO DRUG ANALYSIS
Department of reference Department of Pharmaceutical and Pharmacological Sciences
E-Learning website https://elearning.unipd.it/dsf/course/view.php?idnumber=2015-FA1732-000ZZ-2014-FAO2043780-A1301
Mandatory attendance
Language of instruction Italian
Branch PADOVA
Single Course unit The Course unit CANNOT be attended under the option Single Course unit attendance
Optional Course unit The Course unit is available ONLY for students enrolled in PHARMACY

Lecturers
Teacher in charge VALENTINA GANDIN CHIM/08

ECTS: details
Type Scientific-Disciplinary Sector Credits allocated
Core courses CHIM/08 Pharmaceutical Chemistry 6.0

Course unit organization
Period First semester
Year 2nd Year
Teaching method frontal

Type of hours Credits Teaching
hours
Hours of
Individual study
Shifts
Laboratory 3.0 45 30.0 No turn
Lecture 3.0 24 51.0 No turn

Calendar
Start of activities 01/10/2015
End of activities 28/01/2016
Show course schedule 2019/20 Reg.2018 course timetable

Examination board
Board From To Members of the board
8 Commissione a.a. 2018/19 03/12/2018 30/09/2019 GANDIN VALENTINA (Presidente)
MARZANO CRISTINA (Membro Effettivo)
7 Commissione a.a. 2017/18 01/12/2017 30/09/2018 GANDIN VALENTINA (Presidente)
MARZANO CRISTINA (Membro Effettivo)
DOLMELLA ALESSANDRO (Supplente)
6 Commissione a.a. 2016/17 01/12/2016 30/09/2017 GANDIN VALENTINA (Presidente)
MARZANO CRISTINA (Membro Effettivo)
DOLMELLA ALESSANDRO (Supplente)
MANZINI PAOLO (Supplente)
5 Commissione M-Z a.a. 2015-2016 01/10/2015 30/09/2016 GANDIN VALENTINA (Presidente)
DOLMELLA ALESSANDRO (Membro Effettivo)
MARZANO CRISTINA (Membro Effettivo)
MANZINI PAOLO (Supplente)
MARZARO GIOVANNI (Supplente)
4 Commissione A-L a.a. 2015-2016 01/10/2015 30/09/2016 GANDIN VALENTINA (Presidente)
DOLMELLA ALESSANDRO (Membro Effettivo)
MARZANO CRISTINA (Membro Effettivo)
MANZINI PAOLO (Supplente)
MARZARO GIOVANNI (Supplente)

Syllabus
Prerequisites: Knowledge of general and inorganic chemistry bases; knowledge of the analytical chemistry bases and of the properties of the equilibrium reactions in aqueous solution.
Target skills and knowledge: The course is designed to enable the student to successfully approach the practice experimental chemistry. In particular, the main objectives of the course are to provide an adequate theoretical knowledge and an appropriate modus operandi in the application of simple analytical methods for the analysis of inorganic substances of pharmaceutical interest included in the Italian Official Pharmacopoeia and European Pharmacopoeia. To achieve this, the fundamental principles of the qualitative chemical analysis, particularly with regard to inorganic substances of pharmaceutical interest, are illustrated in the lectures and put into practice in subsequent laboratory exercises.
Examination methods: Written examination and evaluation of laboratory individual tests and reports.
To take the exam the students must have passed the test of "General and Inorganic Chemistry".
Assessment criteria: The assessment of learning for each student will be made ​​either by evaluation of some practical laboratory exercises (single place), either by a written examination. In particular, will be evaluated:
- Knowledge of safety in chemical laboratories.
- Knowledge of the main equipment and laboratory instrumentation.
- Ability to prepare a lab report.
- Knowledge of the theoretical foundations of equilibria in solution from the analytical point of view and application of the same principles to qualitative analytical chemistry.
- Skill in the basic operations of the laboratory.
- Ability to perform qualitative analysis of inorganic substances reported in the FUI.
- Interpretation and rational criticism of the results obtained in the experimental tests carried out in the laboratory.
Course unit contents: -General laboratory chemical safety practices, accident prevention and first aid items.
-Main techniques and basic operations in the practice of experimental chemistry.
-Identification tests for qualitative analysis of inorganic pharmaceuticals
-Analytical methods for the analysis of inorganic substances of pharmaceutical interest inserted in the Italian Official Pharmacopoeia and the European Pharmacopoeia.
Planned learning activities and teaching methods: -Safety practices and safety data sheets in a chemical laboratory; accident prevention and PPE, equipment and safety and emergency signs;
-Theoretical aspects solubilization and precipitation (solubility and solubility product, factors that influence the solubility product, precipitation, relationship between solubility and solubility product, the common ion effect, selective precipitation); acid-base equilibria (definition of acid and base, the fundamental equations for the study of chemical equilibria, pH of solutions); redox equilibria;
-Coordination compounds and their stability as a function of pH. Dissolution of precipitates by complexation;
-Laboratory equipment, analytical techniques and basic operations (measures of weight and volume, solubilization and dilution, preparation of standard solutions, preparation of buffer solutions);
-Introduction to qualitative methods of drug analysis; the analytical signal; Knowledge and application of methods for the qualitative analysis of inorganic drugs included in the Italian Official Pharmacopoeia and in the European Pharmacopoeia.

Theoretical lectures supported by PowerPoint slides and practical laboratory single seat, with the same teacher.
Additional notes about suggested reading: La sicurezza nei laboratori chimici(Progetto, Padova);Regolamento di Sicurezza per gli Studenti dell’Università di Padova; Guida al Laboratorio Propedeutico all’Analisi dei Medicinali (Progetto, PD)
Textbooks (and optional supplementary readings)
  • D.A. Skoog, D.M. West, F.J. Holler, S.R. Crouch, Fondamenti di Chimica Analitica,. --: EdiSES, --. Cerca nel catalogo
  • A.Araneo, Chimica analitica qualitativa. --: Casa Editrice Ambrosiana, --. Cerca nel catalogo