First cycle
degree courses
Second cycle
degree courses
Single cycle
degree courses
School of Science
INDUSTRIAL CHEMISTRY
Course unit
APPLIED ORGANIC CHEMISTRY
SCP3049516, A.A. 2015/16

Information concerning the students who enrolled in A.Y. 2013/14

Information on the course unit
Degree course First cycle degree in
INDUSTRIAL CHEMISTRY (Ord. 2008)
SC1157, Degree course structure A.Y. 2008/09, A.Y. 2015/16
N0
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Number of ECTS credits allocated 6.0
Type of assessment Mark
Course unit English denomination APPLIED ORGANIC CHEMISTRY
Website of the academic structure http://chimicaindustriale.scienze.unipd.it/2012/laurea
Department of reference Department of Chemical Sciences
E-Learning website https://elearning.unipd.it/chimica/course/view.php?idnumber=2015-SC1157-000ZZ-2013-SCP3049516-N0
Mandatory attendance
Language of instruction Italian
Branch PADOVA
Single Course unit The Course unit can be attended under the option Single Course unit attendance
Optional Course unit The Course unit can be chosen as Optional Course unit

Lecturers
Teacher in charge CRISTINA PARADISI CHIM/06

Mutuated
Course unit code Course unit name Teacher in charge Degree course code
SCP3052819 ORGANIC CHEMISTRY 3 CRISTINA PARADISI SC1156

ECTS: details
Type Scientific-Disciplinary Sector Credits allocated
Core courses CHIM/04 Industrial Chemistry 1.0
Core courses CHIM/06 Organic Chemistry 5.0

Course unit organization
Period Second semester
Year 3rd Year
Teaching method frontal

Type of hours Credits Teaching
hours
Hours of
Individual study
Shifts
Laboratory 1.0 12 13.0 2
Lecture 5.0 40 85.0 No turn

Calendar
Start of activities 01/03/2016
End of activities 11/06/2016
Show course schedule 2019/20 Reg.2014 course timetable

Examination board
Board From To Members of the board
1 a.a.2018/19 20/01/2015 30/11/2019 PARADISI CRISTINA (Presidente)
MAROTTA ESTER (Membro Effettivo)

Syllabus
Prerequisites: Organic Chemistry 1, Organic Chemistry 2.
Target skills and knowledge: The course completes the preparation in basic organic chemistry initiated with the preceding two courses. In addition it introduces NMR and mass spectrometry for the identification and structural characterization of organic compounds.
Examination methods: Written exam.
Assessment criteria: Knowledge of the course subjects: level and depth of understanding, clarity and propriety of elaboration. Ability to apply the acquired knowledge to problem solving.
Course unit contents: Part 1: physical methods in organic chemistry.
Nuclear Magnetic Resonance (NMR): introduction of principles and procedures. Proton NMR: chemical equivalence and chemical shift; scalar coupling; spin systems; magnetic equivalence; analysis and interpretation of first order proton NMR spectra; decoupling. Carbon-13 NMR: analysis of broad-band proton decoupled NMR-C-13 spectra.
Mass spectrometry: introduction of principles and instrumentation for electron ionization experiments; isotopes; fragmentation; molecular ion and base peak; characteristic fragmentation reactions of major classes of organic compounds. Exercises of spectra analysis and interpretation.
Part 2: organic chemistry.
Acid-base chemistry of carbonyl compounds; inductive and resonance effects; keto-enol tautomerism; enols and enolates; alfa-halogenation of carbonyl compounds and the haloformic reaction; enolates nucleophilic addition to carbonyl compounds and condensation reactions (aldol reactions, Claisen reaction); synthesis of alfa,beta-unsatured carbonyl compounds; 1,2 and 1,4 nucleophilic addition; Michael addition; Robinson annulation; decarboxylation. Introduction of heterocyclic compounds.
Planned learning activities and teaching methods: 6 CFU: Lectures in class (theory and exercises) with the aid of slides projection.
1 CFU: Laboratory experiment: characterization of unknown compound through chromatographic separation and acquisition and analysis of proton NMR and mass spectra.
Additional notes about suggested reading: All the material used in the lectures (theory and exercises) will be available to the students of the course on the teacher's webpage.
Textbooks (and optional supplementary readings)
  • R. M. Silverstein, F. X. Webster, Identificazione spettroscopica dei composti organici. Milano: Casa Editrice Ambrosiana, 2006. Seconda Edizione Cerca nel catalogo
  • J. Clayden, N. Greeves, S. Warren, P. Wothers, Organic Chemistry. --: Oxford University Press, 2000. Cerca nel catalogo